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doi: 10.17586/2226-1494-2024-24-1-1-10

Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method

A. Moussaoui, D. V. Bulyga, A. I. Ignatiev, S. K. Evstropiev, N. V. Nikonorov


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Article in Russian

For citation:
Moussaoui A., Bulyga D.V., Ignatiev A.I., Evstropiev S.K., Nikonorov N.V. Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method. Scientific and Technical Journal of Information Technologies, Mechanics and Optics, 2024, vol. 24, no. 1, pp. 1–10 (in Russian). doi: 10.17586/2226-1494-2024-24-1-1-10


Abstract
Synthesis of nanocrystalline yttrium-aluminum garnet doped with neodymium was performed via modified Pechini methods. Evolution of material during synthesis was studied using differential thermal analysis; the structure and morphology of synthesized nanopowders were studied using scanning electron microscopy and x-ray diffraction. It was shown that the use of an additional low-temperature stabilizer leads to formation of crystalline yttrium-aluminum garnet phase at lower temperatures. It was shown that the formation of nanocrystals occurs at the temperature of about 883 °C. Obtained powders can be used as precursors for ceramics sintering or be introduced into the optical fiber in order to fabricate optical amplifiers.

Keywords: YAG, luminescence, Pechini method, polyvinylpyrrolidone

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